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PRODUCT DESCRIPTION
Product Code: Single Analyte Atomic Absorption Solution
Catalog Number: AATL1
Lot Number: N2-TL666940
Matrix: 1% (v/v) HNO3
Value / Analyte(s): 1 000 µg/mL
ea: Thallium
CERTIFIED VALUES AND UNCERTAINTIES
Certified Value: 1000 ± 10 μg/mL
Certified Density: 1.005 g/mL (measured at 20 ± 4 ºC)
TRACEABILITY TO NIST
The concentration of this solution standard has been verified by Inductively Coupled Plasma Spectroscopy (ICP) and is traceable to NIST SRM 3158.
1.Thermometer Calibration
-All thermometers are NIST traceable through thermometers that are calibrated by an accredited calibration laboratory.
2.Balance Calibration
-All analytical balances are calibrated by an accredited calibration laboratory and procedure. The weights used for testing are annually compared to master weights and are traceable to NIST.
3.Glassware Calibration
-An in-house procedure is used to calibrate all Class A glassware used in the manufacturing and quality control of CRM/RMs
TRACE METALLIC IMPURITIES (TMI ) DETERMINED BY ICP-MS AND ICP-OES (µg/mL)
N/A
INTENDED USE
For the calibration of analytical instruments and validation of analytical methods as appropriate
NSTRUCTIONS FOR THE CORRECT USE OF THIS REFERENCE MATERIAL
1.Storage and Handling Recommendations
-Store between approximately 4° - 30° C while in sealed TCT bag.
-While stored in the sealed TCT bag, transpiration of this CRM/RM is negligible. After opening the sealed TCT bag transpiration of the CRM/RM will occur, resulting in a gradual increase in the analyte concentration(s). It is the responsibility of the user to account for this effect. When the bottle is weighed both before and after being placed in storage, the mass difference observed will be a measure of transpiration mass loss.
- After opening the sealed TCT bag, keep cap tightly sealed when not in use and store between 4° - 24° C tominimize the effects of transpiration. Use at 20° ± 4° C to minimize volumetric dilution error when using thereported density. Do not pipette from the container. Do not return removed aliquots to container.
Atomic Weight; Valence; Coordination Number; Chemical Form in Solution - 204.38 +16TI (H2O)61+
Chemical Compatibility -Soluble in HCI,HNO3, and H2SO4.Stable with most metals and inorganic anions.The sulfite, thiocyanate and oxalate are moderately soluble; the phosphate and arsenite are slightly solubleand the sulfide is insoluble.
Stability - 2-100 ppb levels stable for months in 1% HNO3 / LDPE container. 1-10,000 ppm solutionschemically stable for years in 2-5% HNO3/LDPE container.
Tl Containing Samples(Preparation and Solution)-Metal (Best dissolved in HN03 which forms chiefy theTI1+ ion.); Oxide (The thallous oxide is readily soluble in water. The thallic oxide requires high levels of acid);Ores (Carbonate fusion in Pt0 followed by HCl dissolution); Organic Matrices (Sulfuriclperoxide digestion ordry ash and dissolution in HCI).
Atomic Spectroscopic Information (ICP-OES D.L.s are given as radial/axial view):
Technique/Line |
Estimated D.L. | Order | Interferences (underlined indicates severe) |
ICP-MS 205amu |
2 ppt |
n/a |
189Os16O |
ICP-OES 190.864nm |
0.04/0.004µg/mL |
V,Ti |
|
ICP-OES 276.787nm |
0.1/0.01µg/mL |
Ta,V,Fe,Cr |
|
ICP-OES 351.924nm |
0.2/0.02 µg/mL |
Th,Ce,Zr |
HAZARDOUS INFORMATION
-Please refer to the Safety Data Sheet for information regarding this CRM/RM.
HOMOGENEITY
-This solution was mixed according to an in-house procedure and is guaranteed to be homogeneous. Homogeneity data indicate that the end user should take a minimum sample size of 0.2 mL to assure homogeneity.
QUALITY STANDARD DOCUMENTATION
1.10CFR50 Appendix B - Nuclear Regulatory Commission
- Domestic Licensing of Production and Utilization Facilities
2.10CFR21 - Nuclear Regulatory Commission
-Reporting defects and Non-Compliance
3.ISO 9001 Quality Management System Registration
-QSR Certificate Number QSR-1034
CERTIFICATION, LOT EXPIRATION AND PERIOD OF VALIDITY
注:以上信息仅供参考,以产品附带证书为准。
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